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EnglishThe reaction of N-methyl-N-tert-butyldimethylsilyltrifluoroacetamide with arginine proceeds with cleavage of the guanidino group, producing a mixture of the tert-butyldimethylsilyl derivatives of ornithine and carbodiimide. These compounds are identified by analysing the reaction mixture using gas chromatography/mass spectrometry. The reaction of N-methyl-N-tert-butyldimethylsilyltrifluoroacetamide with arginine proceeds with cleavage of the guanidino group, producing a mixture of the tert-butyldimethylsilyl derivatives of ornithine and carbodiimide. These compounds are identified by analysing the reaction mixture using gas chromatography/mass spectrometry.
| Titolo: | Transformation of arginine into ornithine during the preparation of its tert-butyldimethylsilyl derivative for analysis by gas chromatography/mass spectrometry. |
| Autori: | |
| Data di pubblicazione: | 1993 |
| Rivista: | |
| Handle: | http://hdl.handle.net/11369/9493 |
| Appare nelle tipologie: | 1.1 Articolo in rivista |
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