A SPME-GCMS method for the determination of a mixture of organophosphorus pesticides (phorate, diazinon, methylparathion, fenitrothion, malathion, fenthion, ethyl-parathion and methidathion) in wine and different fruit juices was developed. The procedure is solvent-free, simple (direct SPME without further sample pre-treatment) and highly sensitive. Estimated LOD and LOQ ranged from 2 to 33 ng/ml and from 7 to 109 ng/ml, respectively, in wine, and from 2 to 90 ng/ml and from 7 to 297 ng/ml, respectively, in fruit juices. LOQ achieved by the present method are almost always below the maximum residue levels recommended by the European legislation.

Solid-Phase Microextraction - Gas Chromatography Mass Spectrometry: a Fast and Simple Screening Method for the Assessment or Organophosphorus Pesticides Residues in Wine and Fruit Juices

QUINTO, MAURIZIO;
2004

Abstract

A SPME-GCMS method for the determination of a mixture of organophosphorus pesticides (phorate, diazinon, methylparathion, fenitrothion, malathion, fenthion, ethyl-parathion and methidathion) in wine and different fruit juices was developed. The procedure is solvent-free, simple (direct SPME without further sample pre-treatment) and highly sensitive. Estimated LOD and LOQ ranged from 2 to 33 ng/ml and from 7 to 109 ng/ml, respectively, in wine, and from 2 to 90 ng/ml and from 7 to 297 ng/ml, respectively, in fruit juices. LOQ achieved by the present method are almost always below the maximum residue levels recommended by the European legislation.
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/11369/5386
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